Name
Voikina Anna Vladimirovna
Scholastic degree
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Academic rank
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Honorary rank
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Organization, job position
Federal State Unitary Enterprise Azov Fisheries Research Institute (FGUP «AzNIIRKH»)
Web site url
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Articles count: 3
The residual amounts of the pesticides in the coastal water of the Azov Sea were studied in spring seasons of 2009-2011. The concentrations of the pollutants were determined and the degree of their danger for hydrobionts was assessed. The concentrations of the pesticides diluted in the water of the Taganrog Bay and the eastern Azov Sea are shown to be lower than the maximum admissible concentrations set for fish-ery reservoirs
Residual amounts of pesticides in the coastal water of the Azov Sea were studied in the spring seasons of 2009–2011. The concentrations of the pollutants were determined and the degree of their danger for hydrobionts was assessed. The concentrations of pesticides diluted in the water of the Taganrog Bay and the eastern Azov Sea are shown to be lower than the maximum admissible concentrations set for fishery ponds
The method has been developed of simultaneous
determination of active ingredients of different kinds
of pesticides in biological tissues (fish liver) by
applying HPLC with ultra-violet detection and the
rapid method of QuEChERS sample preparation. We
defined optimum volume and composition of the
reagents for the extraction, time of centrifugation and
ultrasound treatment, the origin and composition of
sorbents that ensure maximum extraction of the
substances studied and further cleanup of interfering
substances. Acetonitrile was used as a solvent. The
extraction was carried out in the presence of a
buffering mixture - trisodium citrate dihydrate and
disodium citrate hemihydrate. Bondesil PSA bulk
sorbents (alkylated amine containing two amine
functional groups - secondary and primary) and C18E
(reversed-phase sorbent based on silica gel with
grafted octadecylsilane groups were used to purify the
extract from coextractable substances (fats, proteins,
sugars, organic and fatty acids, pigments and other
impurities). The degree of extraction of the analyzed
active ingredients of pesticides from the liver of fish
was 79%. The detectable pesticide concentrations
ranged from 0,4 to 0,97 mg/kg. The relative standard
deviation of the analysis results amounted to 0,01-0,14